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The development and validation of a quantitative analysis method for phenlybutazone in horse serum - VM02138
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Description
Objective :
1). To synthesise a deuterated analogue of phenybutazone to act as internal marker for the quantitative assay;
2). To develop a quantitative LC-MS method for phenylbutazone with a lower limit of quantification of 25 ng/ml in horse serum;
3). To validate the method according to the SANCO Guidelines; and
4). To provide appropriate training documentation and materials to UK laboratories involved in the statutory and non-statutory schemes for testing for veterinary residues.
Justification:
To enable to UK Surveillance programme to comply with EC Regulations.
Intended Use:
An analytical strategy for the regulatory control of phenylbutazone as part of the National Surveillance Programme. |
Project Documents
• Final Report : The development and validation of a quantitative analysis method for phenylbutazone in horse serum
(337k)
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Time-Scale and Cost
From:
2003
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To:
2003
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Cost: £18,540 |
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Contractor / Funded Organisations
HFL Limited |
Keywords
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Fields of Study
Animal Health
Veterinary Medicine |